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research article

Diffraction artefacts from twins and stacking faults, and the mirage of hexagonal, polytypes or other superstructures

Cayron, Cyril  
November 17, 2020
Scripta Materialia

Recently, a hexagonal phase has been reported in high carbon steels in several studies. Here, we show that the electron microscopy results used in these studies were erroneously interpreted. The extra-spots in the diffraction patterns and the odd contrasts in the high resolution images are not those a superstructure but result from double diffraction and streaking effects due to the presence of twins and stacking faults. We point out a similar unfortunate misunderstanding of these effects in papers reporting the existence of a 9R structure in aluminium or copper, or exotic forms of carbon in diamonds.

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Type
research article
DOI
10.1016/j.scriptamat.2020.11.014
Author(s)
Cayron, Cyril  
Date Issued

2020-11-17

Published in
Scripta Materialia
Volume

194

Article Number

113629

Subjects

Electron diffraction

•

transmission electron microscopy

•

metals and alloys

•

crystal structure

•

artefact

Note

This is an Open Access article under the terms of the Creative Commons Attribution License

Editorial or Peer reviewed

REVIEWED

Written at

EPFL

EPFL units
LMTM  
Available on Infoscience
December 7, 2020
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/173912
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