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Diffraction artefacts from twins and stacking faults, and the mirage of hexagonal, polytypes or other superstructures

Cayron, Cyril  
November 17, 2020
Scripta Materialia

Recently, a hexagonal phase has been reported in high carbon steels in several studies. Here, we show that the electron microscopy results used in these studies were erroneously interpreted. The extra-spots in the diffraction patterns and the odd contrasts in the high resolution images are not those a superstructure but result from double diffraction and streaking effects due to the presence of twins and stacking faults. We point out a similar unfortunate misunderstanding of these effects in papers reporting the existence of a 9R structure in aluminium or copper, or exotic forms of carbon in diamonds.

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1-s2.0-S1359646220307417-main.pdf

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http://purl.org/coar/version/c_970fb48d4fbd8a85

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openaccess

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CC BY-NC-ND

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1.49 MB

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58e2cb8b840468655ae5ae6144b5a30d

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