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  4. Deconvoluting cracking mechanisms in fusion processing of steel-copper multi-materials via <i>Operando</i> X-ray characterisation
 
research article

Deconvoluting cracking mechanisms in fusion processing of steel-copper multi-materials via Operando X-ray characterisation

Özsoy, Andaç  
•
Hearn, William A.
•
Gaudez, Steve
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July 10, 2025
Virtual and Physical Prototyping

This study investigates various cracking mechanisms and their prevalence in fusion processing of steel-copper multi-materials using operando X-ray diffraction and imaging during laser powder-bed fusion (LPBF) of 316L-CuCrZr multi-material. During this investigation, three main types of cracking were identified: (i) solidification cracking, (ii) metal-induced embrittlement (MIE), and (iii) liquation cracking. All cracking types are closely related to phase formation during processing and stem from two underlying mechanisms. First, liquid-liquid phase separation (LLPS) and the monotectic reaction in the 316L-CuCrZr system cause two liquids with vastly different solidification ranges to form, leading to solidification cracking. Second, LLPS and the monotectic reaction uniformly distribute Cu-rich liquid between the Fe-rich dendrites, leading to MIE and/or liquation cracking. Conducted based on the insights gained from the operando characterisation, further experiments showed that cracking can be drastically reduced by avoiding phase separation. However, the complete elimination of cracking necessitates chemical alterations in the material feedstock, indicating that while process adjustments can mitigate cracking, they may fail to fully prevent it. These findings serve as a guideline for understanding the underlying causes of cracking in steelcopper multi-materials, how process optimisation can effectively mitigate cracking, and to what extent such adjustments in processing can achieve this outcome.

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Type
research article
DOI
10.1080/17452759.2025.2526798
Author(s)
Özsoy, Andaç  

École Polytechnique Fédérale de Lausanne

Hearn, William A.
Gaudez, Steve
Jeswani, Rijuta
Chen, Yunhui
Rack, Alexander
Hegedüs, Zoltan
Casati, Nicola
Logé, Roland E.  

École Polytechnique Fédérale de Lausanne

Van Petegem, Steven
Date Issued

2025-07-10

Publisher

Informa UK Limited

Published in
Virtual and Physical Prototyping
Volume

20

Issue

1

Article Number

e2526798

Subjects

Multi-material

•

Cracking

•

Additive manufacturing

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Operando X-ray

•

Functionally graded materials (FGM)

Editorial or Peer reviewed

REVIEWED

Written at

EPFL

EPFL units
LMTM  
FunderFunding(s)Grant NumberGrant URL

Board of the Swiss Federal Institutes of Technology

SFA-AM MULTIMAT project

Swiss National Science Foundation

193799

European Union’s Horizon

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Available on Infoscience
July 14, 2025
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/252155
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