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research article
High-resolution and sensitivity through-bond correlations in ultra-fast magic angle spinning (MAS) solid-state NMR
2011
We introduce a new experiment, which makes use of Spin State Selective manipulations to perform sensitive and resolved through-bond correlations in organic and biological solids at high-fields and under ultra-fast MAS. The scheme is the shortest and most sensitive through-bond correlation method introduced so far in solids, yields resolved fingerprints of uniformly (13)C-labeled biomolecules, and constitutes a tool to highlight slight static structural disorder around crystallographically equivalent molecules in microcrystalline samples.
Type
research article
Web of Science ID
WOS:000286327600024
Authors
Bertini, Ivano
•
•
Felli, Isabella C.
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Laage, Segolene
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Lesage, Anne
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Lewandowski, Jozef R.
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Marchetti, Alessandro
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Pierattelli, Roberta
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Pintacuda, Guido
Publication date
2011
Publisher
Published in
Volume
2
Issue
2
Start page
345
End page
348
Peer reviewed
REVIEWED
EPFL units
Available on Infoscience
January 8, 2015
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