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  4. High-resolution and sensitivity through-bond correlations in ultra-fast magic angle spinning (MAS) solid-state NMR
 
research article

High-resolution and sensitivity through-bond correlations in ultra-fast magic angle spinning (MAS) solid-state NMR

Bertini, Ivano
•
Emsley, Lyndon  
•
Felli, Isabella C.
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2011
CHEMICAL SCIENCE

We introduce a new experiment, which makes use of Spin State Selective manipulations to perform sensitive and resolved through-bond correlations in organic and biological solids at high-fields and under ultra-fast MAS. The scheme is the shortest and most sensitive through-bond correlation method introduced so far in solids, yields resolved fingerprints of uniformly (13)C-labeled biomolecules, and constitutes a tool to highlight slight static structural disorder around crystallographically equivalent molecules in microcrystalline samples.

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Type
research article
DOI
10.1039/c0sc00397b
Web of Science ID

WOS:000286327600024

Author(s)
Bertini, Ivano
Emsley, Lyndon  
Felli, Isabella C.
Laage, Segolene
Lesage, Anne
Lewandowski, Jozef R.
Marchetti, Alessandro
Pierattelli, Roberta
Pintacuda, Guido
Date Issued

2011

Publisher

ROYAL SOC CHEMISTRY

Published in
CHEMICAL SCIENCE
Volume

2

Issue

2

Start page

345

End page

348

Editorial or Peer reviewed

REVIEWED

Written at

OTHER

EPFL units
LRM  
Available on Infoscience
January 8, 2015
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/110011
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