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  4. Dynamic Nuclear Polarization Enhanced Solid-State NMR Spectroscopy of Functionalized Metal-Organic Frameworks
 
research article

Dynamic Nuclear Polarization Enhanced Solid-State NMR Spectroscopy of Functionalized Metal-Organic Frameworks

Rossini, Aaron J.  
•
Zagdoun, Alexandre
•
Lelli, Moreno
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2012
Angewandte Chemie International Edition

A matter of minutes: Dynamic nuclear polarization (DNP) is applied to enhance the signal of solid-state NMR spectra of metal-organic framework (MOF) materials. The signal enhancement enables the acquisition of high-quality 1D 13C solid-state NMR spectra, 2D 1H- 13C dipolar HETCOR and 1D 15N solid-state NMR spectra with natural isotopic abundance in experiment times on the order of minutes. MW=microwaves. © 2012 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

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Type
research article
DOI
10.1002/anie.201106030
Web of Science ID

WOS:000298598500015

Author(s)
Rossini, Aaron J.  
Zagdoun, Alexandre
Lelli, Moreno
Canivet, Jerome
Aguado, Sonia
Ouari, Olivier
Tordo, Paul
Rosay, Melanie
Maas, Werner E.
Coperet, Christophe
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Date Issued

2012

Publisher

Wiley-Blackwell

Published in
Angewandte Chemie International Edition
Volume

51

Issue

1

Start page

123

End page

127

Subjects

dynamic nuclear polarization

•

hyperpolarization

•

metal-organic frameworks

•

solid-state NMR spectroscopy

Editorial or Peer reviewed

REVIEWED

Written at

OTHER

EPFL units
LRM  
Available on Infoscience
January 8, 2015
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/109996
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