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  4. Enhanced Quantification for 3D Energy Dispersive Spectrometry: Going Beyond the Limitation of Large Volume of X-Ray Emission
 
research article

Enhanced Quantification for 3D Energy Dispersive Spectrometry: Going Beyond the Limitation of Large Volume of X-Ray Emission

Burdet, Pierre  
•
Hebert, Cecile  
•
Cantoni, Marco  
2014
Microscopy and Microanalysis

This paper presents a method developed to quantify three-dimensional energy dispersive spectrometry (3D EDS) data with voxel size smaller than the volume from which X-rays are emitted. The influence of the neighboring voxels is corrected by applying recursively a complex quantification, improving thereby the accuracy of the quantification of critically small features. The enhanced quantification method is applied to simulated and measured data. A systematic improvement is obtained compared with classical quantification, proving the concept and the prospect of this method.

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Type
research article
DOI
10.1017/S1431927614001688
Web of Science ID

WOS:000345742900026

Author(s)
Burdet, Pierre  
Hebert, Cecile  
Cantoni, Marco  
Date Issued

2014

Publisher

Cambridge University Press

Published in
Microscopy and Microanalysis
Volume

20

Issue

5

Start page

1544

End page

1555

Subjects

energy dispersive X-ray spectrometry

•

focused ion beam

•

tomographic spectral imaging

•

3D chemical analysis

•

3D microanalysis

•

quantification

•

3D image analysis

Note

National Licences

Editorial or Peer reviewed

REVIEWED

Written at

EPFL

EPFL units
CIME  
Available on Infoscience
February 20, 2015
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/111655
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