Repository logo

Infoscience

  • English
  • French
Log In
Logo EPFL, École polytechnique fédérale de Lausanne

Infoscience

  • English
  • French
Log In
  1. Home
  2. Academic and Research Output
  3. Journal articles
  4. Compression testing spherical particles for strength: Theory of the meridian crack test and implementation for microscopic fused quartz
 
research article

Compression testing spherical particles for strength: Theory of the meridian crack test and implementation for microscopic fused quartz

Pejchal, Vaclav
•
Zagar, Goran  
•
Charvet, Raphael
Show more
2017
Journal Of The Mechanics And Physics Of Solids

We show that uniaxial compression testing of spherical particles can give unambiguous access to their tensile strength as governed by surface flaws if one uses pairs of elasto-plastic platens, tailoring their hardness in order to control the relative area of particle-to-platen contact during the test. This eliminates the development of contact microcracks that are typically found to govern particle fracture when hard platens are used. We show that, if the platen materials are well chosen, one can probe a range of stress states for which it is known that particle failure was initiated along the surface, under elevated hoop stress within a region situated remote from the points of load application. Specifically, platens must be chosen such that particles tend to fracture when the ratio of projected contact area radius to particle radius exceeds a specific value that depends on the Poisson ratio of the particles. With fused quartz of Poisson ratio 0.17, this specific ratio value equals 0.65. We demonstrate the approach using microscopic fused quartz spheres 40 +/- 20 gm in diameter as a testbench material; with those particles hardened steel serves as an appropriate platen material. Their strength values are statistically distributed; this is addressed using several platen materials. The resulting bank of data is interpreted using established survival-analysis methods, namely the non-parametric product-limit estimator. We also give a maximum likelihood estimation of the particle strength Weibull distribution parameters derived from the ensemble of data after left-truncation and/or right-censoring of data points situated inside of the range of unambiguous surface fracture strength measurement for each platen material. This gives a Weibull modulus of 6.3 and characteristic strength of 890 MPa for the fused quartz particles. These values are significantly lower than what is produced in high-strength fused quartz fibers of comparable diameter; the difference is most likely a result of surface damage caused during powder storage and manipulation in the absence of a protective coating.

  • Files
  • Details
  • Metrics
Type
research article
DOI
10.1016/j.jmps.2016.11.009
Web of Science ID

WOS:000393241100005

Author(s)
Pejchal, Vaclav
Zagar, Goran  
Charvet, Raphael
Denereaz, Cyril
Mortensen, Andreas  
Date Issued

2017

Published in
Journal Of The Mechanics And Physics Of Solids
Volume

99

Start page

70

End page

92

Subjects

Uniaxial compression

•

Powder particles

•

Fused quartz

•

Local strength

•

Survival-analysis

Editorial or Peer reviewed

REVIEWED

Written at

EPFL

EPFL units
LMM  
Available on Infoscience
March 27, 2017
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/135924
Logo EPFL, École polytechnique fédérale de Lausanne
  • Contact
  • infoscience@epfl.ch

  • Follow us on Facebook
  • Follow us on Instagram
  • Follow us on LinkedIn
  • Follow us on X
  • Follow us on Youtube
AccessibilityLegal noticePrivacy policyCookie settingsEnd User AgreementGet helpFeedback

Infoscience is a service managed and provided by the Library and IT Services of EPFL. © EPFL, tous droits réservés