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  4. Structural and electroacoustic studies of AIN thin films during low temperature radio frequency sputter deposition
 
research article

Structural and electroacoustic studies of AIN thin films during low temperature radio frequency sputter deposition

Engelmark, F.
•
Iriarte, G. F.
•
Katardjiev, I. V.
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2001
Journal of Vacuum Science & Technology A

AIN is a material used in a wide variety of applications such as electroacoustic devices, blue diodes, IR windows, thermal conductors, metal-insulator-semiconductor structures, integrated circuit packaging, etc. In this work thin piezoelectric AIN polycrystalline films have been grown on Si and SiO2 using rf magnetron sputter deposition in an Ar/N-2 gas mixture. The structural properties of the film have been optimized by varying the deposition parameters, such as process pressure, gas mixture, substrate temperature, discharge power, etc. [K. Tominaga et al., Jpn. J. Appl. Phys., Part 1 35, 4972 (1996); H. Okana et al., ibid. 31, 3446 (1992); K. Kazuya, T. Hanabusa, and K. Tominaga, Thin Solid Films 281-282, 340 (1996)]. It was found that the best film texture was obtained for a particular set of parameters, namely process pressure of 4 mTorr, substrate temperature 350 degreesC, discharge power 350 W, and a gas mixture of 25% Ar and 75% N-2. The films as examined by x-ray diffraction exhibited a columnar structure with a strong (001) texture, and a fall width at half maximum (FWHM) rocking curve of 1.6 degrees. Atomic force microscopy measurements indicated a surface roughness with a rms value of 8 Angstrom. Classical nonapodized transversal surface acoustic wave filters operating at a frequency of 534 MHz were fabricated to characterize the electroacoustic properties of the films. The measurements indicated a coupling coefficient of 0.37% and a phase velocity of 4900 m/s. Further, thin epitaxial films were grown on (001)alpha -Al2O3 (sapphire) under the same deposition conditions except the substrate temperature. The films exhibited a (001)AlN//(001)alpha -Al2O3 plane orientation with a (002) rocking curve FWHM value of about 0.4 degrees, showing a relatively good alignment of the c axis. The in-plane orientation was [110]AlN//[120]alpha -Al2O3 corresponding to a rotation of the AIN film of 30 degrees with respect to the (001)alpha -Al2O3 surface. Cross-sectional transmission electron microscopy studies indicated a population of both thread and edge dislocations with decreasing concentrations with film thickness. (C) 2001 American Vacuum Society.

  • Details
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Type
research article
DOI
10.1116/1.1399320
Author(s)
Engelmark, F.
Iriarte, G. F.
Katardjiev, I. V.
Ottosson, M.
Muralt, P.  
Berg, S.
Date Issued

2001

Published in
Journal of Vacuum Science & Technology A
Volume

19

Issue

5

Start page

2664

End page

2669

Subjects

chemical-vapor-deposition

•

acoustic-wave properties

•

alcl3-nh3 system

•

aluminum nitride

•

aln films

•

orientation

Note

Engelmark, F Univ Uppsala, Angstrom Lab, Box 534, S-75121 Uppsala, Sweden Univ Uppsala, Angstrom Lab, S-75121 Uppsala, Sweden

478YP

Cited References Count:20

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REVIEWED

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LC  
Available on Infoscience
August 21, 2006
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/233447
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