Separation of dipolar and quadrupolar splittings in single crystal nitrogen-14 NMR

A new 2-dimensional Fourier technique is proposed to unravel overlapping resonances in single crystal 14N spectra due to proton-N dipolar couplings. One frequency domain is reserved for the proton decoupled quadrupolar spectrum, while the orthogonal frequency dimension shows the dipolar splittings alone, the quadrupolar interaction being eliminated by refocusing. [on SciFinder (R)]


Published in:
Chemical Physics Letters, 67, 2-3, 424-7
Year:
1979
Laboratories:




 Record created 2006-02-22, last modified 2018-03-17


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