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  4. Dislocation Hardening in a New Manufacturing Route of Ferritic Oxide Dispersion-Strengthened Fe-14Cr Cladding Tube
 
research article

Dislocation Hardening in a New Manufacturing Route of Ferritic Oxide Dispersion-Strengthened Fe-14Cr Cladding Tube

Salliot, Freddy
•
Borbely, Andras
•
Sornin, Denis
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March 1, 2024
Materials

The microstructure evolution associated with the cold forming sequence of an Fe-14Cr-1W-0.3Ti-0.3Y2O3 grade ferritic stainless steel strengthened by dispersion of nano oxides (ODS) was investigated. The material, initially hot extruded at 1100 degrees C and then shaped into cladding tube geometry via HPTR cold pilgering, shows a high microstructure stability that affects stress release heat treatment efficiency. Each step of the process was analyzed to better understand the microstructure stability of the material. Despite high levels of stored energy, heat treatments, up to 1350 degrees C, do not allow for recrystallization of the material. The Vickers hardness shows significant variations along the manufacturing steps. Thanks to a combination of EBSD and X-ray diffraction measurements, this study gives a new insight into the contribution of statistically stored dislocation (SSD) recovery on the hardness evolution during an ODS steel cold forming sequence. SSD density, close to 4.1015 m-2 after cold rolling, drops by only an order of magnitude during heat treatment, while geometrically necessary dislocation (GND) density, close to 1.1015 m-2, remains stable. Hardness decrease during heat treatments appears to be controlled only by the evolution of SSD.

  • Details
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Type
research article
DOI
10.3390/ma17051146
Web of Science ID

WOS:001182790100001

Author(s)
Salliot, Freddy
Borbely, Andras
Sornin, Denis
Loge, Roland E.  

EPFL

Spartacus, Gabriel
Leguy, Hadrien
Baudin, Thierry
de Carlan, Yann
Date Issued

2024-03-01

Publisher

MDPI

Published in
Materials
Volume

17

Issue

5

Article Number

1146

Subjects

Physical Sciences

•

Technology

•

Ods Steel

•

Microstructure

•

Cold Rolling

•

Dislocation Density

•

X-Ray Diffraction

•

Ebsd

Editorial or Peer reviewed

REVIEWED

Written at

EPFL

EPFL units
LMTM  
FunderGrant Number

PX Group to the LMTM laboratory

Available on Infoscience
April 17, 2024
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/207205
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