Repository logo

Infoscience

  • English
  • French
Log In
Logo EPFL, École polytechnique fédérale de Lausanne

Infoscience

  • English
  • French
Log In
  1. Home
  2. Academic and Research Output
  3. Journal articles
  4. The 2D MAS NMR spin-echo experiment: the determination of C-13-C-13 J couplings in a solid-state cellulose sample
 
research article

The 2D MAS NMR spin-echo experiment: the determination of C-13-C-13 J couplings in a solid-state cellulose sample

Brown, SP
•
Emsley, L  
2004
Journal of Magnetic Resonance

A simple C-13 MAS spin-echo experiment is applied to a partially C-13-labelled cellulose sample extracted from wood. C-13-C-13 J couplings are determined even though considerable chemical disorder leads to observed linewidths in the normal 1D C-13 CP MAS spectrum which far exceed the J couplings. The fitting of the experimental data also allows the quantification of the degree of isotopic enrichment. (C) 2004 Elsevier Inc. All rights reserved.

  • Details
  • Metrics
Type
research article
DOI
10.1016/j.jmr.2004.07.022
Web of Science ID

WOS:000225045200009

Author(s)
Brown, SP
Emsley, L  
Date Issued

2004

Publisher

Academic Press Inc - Elsevier Science

Published in
Journal of Magnetic Resonance
Volume

171

Issue

1

Start page

43

End page

47

Subjects

MAS

•

spin-echo

•

J couplings

•

cellulose

•

C-13

Editorial or Peer reviewed

REVIEWED

Written at

OTHER

EPFL units
LRM  
Available on Infoscience
January 8, 2015
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/110095
Logo EPFL, École polytechnique fédérale de Lausanne
  • Contact
  • infoscience@epfl.ch

  • Follow us on Facebook
  • Follow us on Instagram
  • Follow us on LinkedIn
  • Follow us on X
  • Follow us on Youtube
AccessibilityLegal noticePrivacy policyCookie settingsEnd User AgreementGet helpFeedback

Infoscience is a service managed and provided by the Library and IT Services of EPFL. © EPFL, tous droits réservés