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research article
Measurement of Site-Specific C-13 Spin-Lattice Relaxation in a Crystalline Protein
We demonstrate that it is possible to record site-specific spin-lattice relaxation rates for the majority of C-13 sites in uniformly C-13 and N-15 labeled solid proteins as a result of the slowing down of proton-driven spin diffusion at sample spinning frequencies >= 60 kHz, thus providing a series of new experimental probes for characterizing molecular dynamics in solid proteins.
Type
research article
Web of Science ID
WOS:000278905700013
Authors
Lewandowski, Jozef R.
•
Sein, Julien
•
Sass, Hans Juergen
•
Grzesiek, Stephan
•
Blackledge, Martin
•
Publication date
2010
Publisher
Published in
Volume
132
Issue
24
Start page
8252
End page
8254
Peer reviewed
REVIEWED
EPFL units
Available on Infoscience
January 8, 2015
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