research article
Molecular-level characterization of the structure and the surface chemistry of periodic mesoporous organosilicates using DNP-surface enhanced NMR spectroscopy
We present the molecular level characterization of a phenylpyridine-based periodicmesoporous organosilicate and its post-functionalized organometallic derivatives through the fast acquisition of high quality natural isotopic abundance 1D C-13, N-15, and Si-29 and 2D 1H-C-13 and 1H-Si-29 solid-state NMR spectra enhanced with dynamic nuclear polarization.
Type
research article
Web of Science ID
WOS:000322401600005
Author(s)
Gruening, Wolfram R.
Zagdoun, Alexandre
Gajan, David
Lesage, Anne
Coperet, Christophe
Date Issued
2013
Publisher
Published in
Volume
15
Issue
32
Start page
13270
End page
13274
Editorial or Peer reviewed
REVIEWED
Written at
OTHER
EPFL units
Available on Infoscience
January 8, 2015
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