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research article
Molecular-level characterization of the structure and the surface chemistry of periodic mesoporous organosilicates using DNP-surface enhanced NMR spectroscopy
We present the molecular level characterization of a phenylpyridine-based periodicmesoporous organosilicate and its post-functionalized organometallic derivatives through the fast acquisition of high quality natural isotopic abundance 1D C-13, N-15, and Si-29 and 2D 1H-C-13 and 1H-Si-29 solid-state NMR spectra enhanced with dynamic nuclear polarization.
Type
research article
Web of Science ID
WOS:000322401600005
Authors
Gruening, Wolfram R.
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Zagdoun, Alexandre
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Gajan, David
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Lesage, Anne
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Coperet, Christophe
Publication date
2013
Publisher
Published in
Volume
15
Issue
32
Start page
13270
End page
13274
Peer reviewed
REVIEWED
EPFL units
Available on Infoscience
January 8, 2015
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