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research article
Cross polarization from H-1 to quadrupolar Li-6 nuclei for dissolution DNP
Cross polarization from protons to quadrupolar Li-6 nuclei is combined with dynamic nuclear polarization of protons at 1.2 K and 6.7 T using TEMPOL as a polarizing agent followed by rapid dissolution. Compared to direct Li-6 DNP without cross-polarization, a higher nuclear spin polarization P(Li-6) can be obtained in a shorter time. A double resonance H-1-Li-6 probe was designed that is equipped for Longitudinally Detected Electron Spin Resonance.
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Name
P386-Perez-Linde-Bornet-Milani-Vuichoud-Melzi-Jannin-Bodenhausen-CP-1H-6Li-D-DNP-PCCP-16-24813-2014.pdf
Access type
openaccess
Size
1.85 MB
Format
Adobe PDF
Checksum (MD5)
496745fba1f8b2fb913875473cf2d605