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research article

Fast in-situ annealing stage coupled with EBSD: A suitable tool to observe quick recrystallization mechanisms

Bozzolo, N.
•
Jacomet, S.
•
Logé, R.E.  
2012
Materials Characterization

A heating stage has been developed to perform in-situ annealing in a SEM equipped with an EBSD system in order to study recrystallization mechanisms. High temperature treatments could then be performed inside the SEM, up to 1180°C and with high heating and cooling rates (∼ 100°C s - 1). Samples were cooled down to room temperature to perform EBSD orientation mapping in between successive short-duration heat treatments. Microstructure evolution snapshots obtained this way allow gaining an insight into recrystallization mechanisms. The interest of such experiments is shown for two examples: static recrystallization of cold deformed pure tantalum and post-dynamic evolution of hot-deformed Zircaloy4. © 2012 Elsevier Inc. All rights reserved.

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Type
research article
DOI
10.1016/j.matchar.2012.04.020
Author(s)
Bozzolo, N.
•
Jacomet, S.
•
Logé, R.E.  
Date Issued

2012

Published in
Materials Characterization
Volume

70

Start page

28

End page

32

Subjects

Annealing

•

crystallization

•

Dynamic recrystallization

•

EBSD

•

Heating and cooling rates

•

Heating stage

•

High temperature treatments

•

In-situ annealing

•

Microstructure evolutions

•

Orientation mapping

•

Recrystallization

•

Recrystallization mechanisms

•

Room temperature

•

Static recrystallization

•

Tantalum

•

Zircaloy-4

•

Zirconium

Peer reviewed

REVIEWED

Written at

OTHER

EPFL units
LMTM  
Available on Infoscience
November 14, 2014
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/108762
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