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  4. EBSD coupled to SEM in situ annealing for assessing recrystallization and grain growth mechanisms in pure tantalum
 
research article

EBSD coupled to SEM in situ annealing for assessing recrystallization and grain growth mechanisms in pure tantalum

Kerisit, C.
•
Logé, R.E.  
•
Jacomet, S.
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2013
Journal of Microscopy

An in situ annealing stage has been developed in-house and integrated in the chamber of a Scanning Electron Microscope equipped with an Electron BackScattered Diffraction system. Based on the Joule effect, this device can reach the temperature of 1200°C at heating rates up to 100°C/s, avoiding microstructural evolutions during heating. A high-purity tantalum deformed sample has been annealed at variable temperature in the range 750°C-1030°C, and classical mechanisms of microstructural evolutions such as recrystallization and grain coarsening phenomena have been observed. Quantitative measurements of grain growth rates provide an estimate of the mean grain boundary mobility, which is consistent with the value estimated from physical parameters reported for that material. In situ annealing therefore appears to be suited for complementing bulk measurements at relatively high temperatures, in the context of recrystallization and grain growth in such a single-phase material. © 2013 The Authors Journal of Microscopy © 2013 Royal Microscopical Society.

  • Details
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Type
research article
DOI
10.1111/jmi.12034
Author(s)
Kerisit, C.
Logé, R.E.  
Jacomet, S.
Llorca, V.
Bozzolo, N.
Date Issued

2013

Published in
Journal of Microscopy
Volume

250

Start page

189

End page

199

Subjects

article

•

crystallization

•

EBSD

•

electron back scattered diffraction

•

electron diffraction

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grain

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Grain boundary mobility

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Grain growth

•

growth

•

growth rate

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heating

•

in situ

•

molecular evolution

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nonhuman

•

physical parameters

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priority journal

•

quantitative analysis

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scanning electron microscopy

•

Static recrystallization

•

Tantalum

•

temperature

Editorial or Peer reviewed

REVIEWED

Written at

OTHER

EPFL units
LMTM  
Available on Infoscience
November 14, 2014
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/108756
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