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research article

Electron microscopy of biomaterials based on hydroxyapatite

Suvorova, E. I.  
•
Klechkovskaya, V. V.
•
Komarov, V. F.
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2006
Crystallography Reports

Three types of biomaterials based on hydroxyapatite are synthesized and investigated. Hydroxyapatite nanocrystals or microcrystals precipitated from low-temperature aqueous solutions serve as the initial material used for preparing spherical porous granules approximately 300-500 mu m in diameter. Sintering of hydroxyapatite crystals at a temperature of 870 degrees C for 2 h or at 1000 degrees C (for 3 h) + 1200 degrees C (for 2 h) brings about the formation of solid ceramics with different internal structures. According to the electron microscopic data, the ceramic material prepared at 870 degrees C is formed by agglomerated hydroxyapatite nanocrystals, whereas the ceramics sintered at 1200 degrees C (with a bending strength of the order of 100 MPa) are composed of crystal blocks as large as 2 mu m. It is established that all the biomaterials have a single-phase composition and consist of the hydroxyapatite with a structure retained up to a temperature of 1200 degrees C.

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Type
research article
DOI
10.1134/S1063774506050191
Web of Science ID

WOS:000240807000019

Author(s)
Suvorova, E. I.  
Klechkovskaya, V. V.
Komarov, V. F.
Severin, A. V.
Melikhov, I. V.
Buffat, P. A.  
Date Issued

2006

Published in
Crystallography Reports
Volume

51

Issue

5

Start page

881

End page

887

Subjects

Diffraction

•

Phosphate

•

Delivery

•

Implants

Editorial or Peer reviewed

REVIEWED

Written at

EPFL

EPFL units
CIME  
Available on Infoscience
October 12, 2008
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/30244
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