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  4. The effect of three-fold astigmatism on measurements of grain boundary volume expansion by high-resolution transmission electron microscopy
 
research article

The effect of three-fold astigmatism on measurements of grain boundary volume expansion by high-resolution transmission electron microscopy

Merkle, KL
•
Csencsits, R
•
Rynes, KL
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1998
Journal of Microscopy

In the absence of high-order aberrations, the lattice fringe technique should allow measurement of grain boundary rigid-body displacements to accuracies about an order of magnitude better than the point-to-point resolution of the transmission electron microscope. The three-fold astigmatism, however, introduces shifts of the lattice fringe pattern that depend on the orientation of the lattice relative to the direction of the three-fold astigmatism and thus produces an apparent shift between the two grains bordering the grain boundary. By image simulation of grain boundary model structures, the present paper explores the effect of these extraneous shifts on grain boundary volume expansion measurements. It is found that the shifts depend, among others, on zone axis direction and the magnitude of the lattice parameter. For many grain boundaries of interest, three-fold astigmatism correction to better than 100 nm appears necessary to achieve the desired accuracies.

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Type
research article
DOI
10.1046/j.1365-2818.1998.2890841.x
Author(s)
Merkle, KL
•
Csencsits, R
•
Rynes, KL
•
Withrow, JP
•
Stadelmann, PA  
Date Issued

1998

Published in
Journal of Microscopy
Volume

190

Issue

1-2

Start page

204

End page

13

Editorial or Peer reviewed

REVIEWED

Written at

EPFL

EPFL units
CIME  
Available on Infoscience
February 15, 2007
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/2936
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