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research article

Optimal aperture sizes and positions for EMCD experiments

Verbeeck, J.
•
Hébert, C.  
•
Rubino, S.
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2008
Ultramicroscopy

The signal-to-noise ratio (SNR) in energy-loss magnetic chiral dichroism (EMCD)-the equivalent of X-ray magnetic circular dichroism (XMCD) in the electron microscope-is optimized with respect to the detector shape, size and position. We show that an important increase in SNR over previous experiments can be obtained when taking much larger detector sizes. We determine the ideal shape of the detector but also show that round apertures are a good compromise if placed in their optimal position. We develop the theory for a simple analytical description of the EMCD experiment and then apply it to dynamical multibeam Bloch wave calculations and to an experimental data set. In all cases it is shown that a significant and welcome improvement of the SNR is possible.

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Type
research article
DOI
10.1016/j.ultramic.2008.02.007
Web of Science ID

WOS:000258747600009

Author(s)
Verbeeck, J.
Hébert, C.  
Rubino, S.
Novak, P.
Rusz, J.
Houdellier, F.
Gatel, C.
Schattschneider, P.
Date Issued

2008

Publisher

Elsevier

Published in
Ultramicroscopy
Volume

108

Issue

9

Start page

865

End page

872

Subjects

Circular dichroism

•

Coherence

•

Electron energy loss spectrometry

•

Transmission electron microscopy

Editorial or Peer reviewed

REVIEWED

Written at

EPFL

EPFL units
LSME  
CIME  
Available on Infoscience
February 17, 2009
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/35389
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