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  4. A miniaturized selective laser melting device for operando X-ray diffraction studies
 
research article

A miniaturized selective laser melting device for operando X-ray diffraction studies

Hocine, Samy  
•
Van Petegem, Steven
•
Frommherz, Ulrich
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August 1, 2020
Additive Manufacturing

We report on the development of a miniaturized device for operando X-ray diffraction during laser 3D printing. The printing chamber has a size of only 130 x 135 x 34 mm(3) and is optimized to be installed at synchrotron beamlines. We describe the design considerations, details on the setup and the implementation at two different beamlines of the Swiss Light Source. Its capabilities are demonstrated by ex situ printing of complex shapes and operando X-ray diffraction experiments using Ti-6Al-4V powder. It is shown that the beamline characteristics have an important influence on the X-ray footprints of the microstructural evolution during 3D printing. From the intensity of the diffraction peaks, the evolution of the different phases can be followed during printing. Furthermore, the diffuse scattering signal provides information on the precise location of the laser beam on the sample and the scanning head settling time.

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Type
research article
DOI
10.1016/j.addma.2020.101194
Web of Science ID

WOS:000555840800006

Author(s)
Hocine, Samy  
Van Petegem, Steven
Frommherz, Ulrich
Tinti, Gemma
Casati, Nicola
Grolimund, Daniel
Van Swygenhoven, Helena  
Date Issued

2020-08-01

Publisher

ELSEVIER

Published in
Additive Manufacturing
Volume

34

Article Number

101194

Subjects

Engineering, Manufacturing

•

Materials Science, Multidisciplinary

•

Engineering

•

Materials Science

•

powder bed fusion

•

operando x-ray diffraction

•

ti alloys

•

phase evolution

•

phase-field

Editorial or Peer reviewed

REVIEWED

Written at

EPFL

EPFL units
UPSWYG  
Available on Infoscience
August 19, 2020
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/170925
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