Improved heteronuclear decoupling schemes for solid-state magic angle spinning NMR by direct spectral optimization

De Paepe, GHodgkinson, PEmsley, L2015-01-082015-01-082015-01-08200310.1016/S0009-2614(03)00966-7https://infoscience.epfl.ch/handle/20.500.14299/110108WOS:000185168000001It is shown that a direct spectral optimization scheme can be implemented to obtain improved heteronuclear dipolar decoupling schemes for solid-state magic-angle-spinning NMR experiments. The resulting schemes, which turn out to have a particularly simple form, are shown to be applicable over the whole range of commercially available spinning speeds (from 5 to 35 kHz), and are shown to improve on the performance of the best existing sequences. (C) 2003 Elsevier Science B.V. All rights reserved.Improved heteronuclear decoupling schemes for solid-state magic angle spinning NMR by direct spectral optimizationtext::journal::journal article::research article