Direct conversion of alkyl thiols to the corresponding sulfonyl fluorides

RSH (R = n-octyl, cyclohexyl, tert-nonyl) were oxidized by NO2 in >=65% aq. HF to give RSO2F in ?85% yields. [on SciFinder (R)]


Published in:
Synthesis, 12, 887
Year:
1974
Laboratories:




 Record created 2006-02-22, last modified 2018-03-17


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