In situ X-ray diffraction experiments on lithium intercalation compounds

We describe powder X-ray diffraction experiments on lithium intercalation compounds. Using a unique electrochemical cell which incorporates a beryllium X-ray window we are able to monitor changes in the host lattice which occur when the lithium concentration is altered electrochemically. The detailed design of the cells and experimental problems which arise when using the in situ X-ray diffraction technique are discussed. Results of experiments on LixTiS2 are reported for 0<x<2.


Published in:
Canadian Journal of Physics, 60, 3, 307-313
Year:
1982
Publisher:
National Research Council Canada
ISSN:
0008-4204
Keywords:
Laboratories:




 Record created 2015-08-28, last modified 2018-03-17


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