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  4. In-situ selective laser heat treatment for microstructural control of additively manufactured Ti-6Al-4V
 
research article

In-situ selective laser heat treatment for microstructural control of additively manufactured Ti-6Al-4V

Esmaeilzadeh, Reza  
•
Hamidi-Nasab, Milad  
•
de Formanoir, Charlotte  
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November 23, 2023
Additive Manufacturing

As-built Laser Powder Bed Fusion (LPBF) Ti-6Al-4V typically exhibits a fully acicular alpha '-martensite microstructure, and requires post-process heat treatment in order to decompose the martensite and achieve sufficient ductility. In the present study, we demonstrate a simple concept based on in-situ Selective Laser Heat Treatment (SLHT) that can effectively alter the microstructure and activate the decomposition of the alpha '-martensite into a lamellar alpha +beta microstructure within a short time scale (similar to 30 s). SLHT consists of multiple rescanning of the printed part, with low energy density, triggering solid-state phase transformations. Operando X-ray diffraction has been performed on cuboid and thin wall geometries, and was augmented by thermal finite element simulations. Upon SLHT, a gradual formation of the beta phase as well as an alpha/ peak narrowing trend have been evidenced through X-ray diffraction, as an indication of the diffusional nature of alpha '-martensite decomposition. Moreover, through fine tuning of the process parameters at the final stage of SLHT, a controlled temperature evolution during cooling was achieved, leading to preservation of the beta phase, a product of the decomposition, down to room temperature. Complementary microstructural characterizations via EBSD, SEM, and TEM confirm the presence of a lamellar alpha +beta microstructure after SLHT. Our results evidence, for the first time, the fast kinetics of alpha '-martensite decomposition under in-situ SLHT. The approach is meant to be implemented at selected locations during the LPBF process, avoiding time-consuming post processing steps, and leading to composite-like, architected microstructures.

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Type
research article
DOI
10.1016/j.addma.2023.103882
Web of Science ID

WOS:001125764800001

Author(s)
Esmaeilzadeh, Reza  
Hamidi-Nasab, Milad  
de Formanoir, Charlotte  
Schlenger, Lucas Maximilian  
Van Petegem, Steven
Navarre, Claire  
Cayron, Cyril  
Casati, Nicola
Grolimund, Daniel
Loge, Roland E.  
Date Issued

2023-11-23

Publisher

Elsevier

Published in
Additive Manufacturing
Volume

78

Article Number

103882

Subjects

Technology

•

Laser Powder Bed Fusion (Lpbf)

•

Selective Laser Heat Treatment (Slht)

•

Martensite Decomposition

•

Operando X-Ray Diffraction

•

Finite Element Simulation (Fem)

Editorial or Peer reviewed

REVIEWED

Written at

EPFL

EPFL units
LMTM  
FunderGrant Number

Swiss National Science Foundation (SNSF)

CRSII5_193799

PX-group

Available on Infoscience
February 20, 2024
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/204773
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