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research article

Low-power decoupling at high spinning frequencies in high static fields

Weingarth, Markus
•
Bodenhausen, Geoffrey  
•
Tekely, Piotr
2009
Journal of Magnetic Resonance

We demonstrate that heteronuclear decoupling using a Phase-Inverted Supercycled Sequence for Attenuation of Rotary Resonance (PISSARRO) is very efficient at high spinning frequencies (v(rot) = 60 kHz) and high magnetic fields (900 MHz for protons at 21 T) even with moderate radio-frequency decoupling amplitudes (v(1)' = 15 kHz), despite the wide range of isotropic chemical shifts of the protons and the increased effect of their chemical shift anisotropy. (C) 2009 Elsevier Inc. All rights reserved.

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Type
research article
DOI
10.1016/j.jmr.2009.04.015
Author(s)
Weingarth, Markus
Bodenhausen, Geoffrey  
Tekely, Piotr
Date Issued

2009

Publisher

Academic Press Inc - Elsevier Science

Published in
Journal of Magnetic Resonance
Volume

199

Start page

238

End page

241

Subjects

Low-power heteronuclear decoupling

•

Fast MAS

•

Nuclear-Magnetic-Resonance

•

Rotary Resonance

•

Rotating Solids

•

Nmr Experiments

•

Sequence

Editorial or Peer reviewed

NON-REVIEWED

Written at

OTHER

EPFL units
LRMB  
Available on Infoscience
June 3, 2010
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/50625
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