Synthesis, characterization and X-ray crystal structures of lithium coordination polymer from cyclobutane-1,1-dicarboxylic acid

Chen, Z; Fei, Z; Zhao, D; Feng, Y; Yu, K

doi:10.1016/j.inoche.2006.09.013

research article

Synthesis, characterization and X-ray crystal structures of lithium coordination polymer from cyclobutane-1,1-dicarboxylic acid

Chen, Z

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Fei, Z

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Zhao, D

more

2007

INORGANIC CHEMISTRY COMMUNICATIONS

A novel lithium salt, cyclobutane-1,1-dicarboxylic lithium was synthesized and characterized by NMR, IR, ESI-MS, X-ray single crystal analysis, and TG/DTG (TGA) thermal analysis. The crystal structure information reveals the coordination polymer nature and ESI-MS shows its aggregation behavior in aqueous solution. TGA analysis discloses the CO<sub>2</sub> release with respect to temperature rise.