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research article
Accurate determination of scalar couplings by convolution of complementary two-dimensional multiplets
The authors describe how the value of a nuclear spin coupling const. JAX can be detd. very accurately by comparing 2 complementary 2-dimensional multiplets obtained with selective correlation NMR spectroscopy (soft-COSY) and with pure in-phase correlation spectroscopy. The convolution method of J. J. Titman and J. Keeler (1990) was adapted to compare soft-COSY and PICSY multiplets. Illustrative results on the L-proline residue in cyclo-(L-Pro1-L-Pro2-D-Pro3) are presented. [on SciFinder (R)]
Type
research article
Authors
Publication date
1993
Published in
Volume
103
Issue
1
Start page
118
End page
21
Peer reviewed
REVIEWED
EPFL units
Available on Infoscience
February 22, 2006
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