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  4. Effect of ion-irradiation on the microstructure and microhardness of the W-2Y(2)O(3) composite materials fabricated by sintering and hot forging
 
conference paper

Effect of ion-irradiation on the microstructure and microhardness of the W-2Y(2)O(3) composite materials fabricated by sintering and hot forging

Battabyal, M.
•
Spätig, P.
•
Baluc, N.
2013
Fusion Engineering And Design
27th Symposium on Fusion Technology (SOFT)

A W-2Y(2)O(3) material was developed in collaboration with the Plansee Company (Austria). An ingot of the material having approximate dimension of 95 mm x 20 mm was fabricated by mixing the elemental powders followed by pressing, sintering and hot forging. The microstructure of the W-2Y(2)O(3) composite was investigated using transmission electron microscopy (TEM). The microhardness wasostudied using nano-indentation technique. We observed that the W-grains having a mean size of about 1 mu m already formed and these grains contain very low density of dislocations. The size of the yttria particles was between 300 nm and 1 mu m and the Berkovich hardness was about 4.8 GPa. The specimens were irradiated/implanted with Fe and He ions at JANNuS facility located at Orsay/Saclay, France. The TEM disks kept were irradiated/implanted at 300 and 700 degrees C using Fe and He ions with an energy of 24 and 2 MeV, respectively. The calculated radiation dose was about 5 dpa produced by Fe ions and total He content is 75 appm at both 300 and 700 degrees C. From the TEM investigation of irradiated samples, few radiation loops are present on the W grains, whereas on yttria particles, the radiation induced damages appear as voids. Berkovich hardness of the irradiated sample is higher than that of the non-irradiated sample. Results on the microstructure and microhardness of the ion-irradiated W-2Y(2)O(3) composites are presented in detail. (C) 2013 Elsevier B.V. All rights reserved.

  • Details
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Type
conference paper
DOI
10.1016/j.fusengdes.2013.03.060
Web of Science ID

WOS:000326903200047

Author(s)
Battabyal, M.
Spätig, P.
Baluc, N.
Date Issued

2013

Publisher

Elsevier Science Sa

Publisher place

Lausanne

Published in
Fusion Engineering And Design
Total of pages

5

Volume

88

Issue

9-10

Start page

1668

End page

1672

Subjects

Tungsten

•

Yttria

•

Irradiation

•

Microhardness

•

Transmission electron microscopy

Editorial or Peer reviewed

REVIEWED

Written at

EPFL

EPFL units
CRPP  
SPC  
Event name
27th Symposium on Fusion Technology (SOFT)
Available on Infoscience
January 9, 2014
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/99369
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