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research article

Cold neutron diffraction contrast tomography of polycrystalline material

Peetermans, S.
•
King, A.
•
Ludwig, W.
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2014
Analyst

Traditional neutron imaging is based on the attenuation of a neutron beam through scatteririg and absorption upon traversing a sample of interest. It offers insight into the sample's material distribution at high spatial resolution in a non-destructive way. In this work, it is expanded to include the diffracted neutrons that were ignored so far and obtain a crystallographic distribution (grain mapping). Samples are rotated in a cold neutron beam of limited wavelength band. Projections of the crystallites formed by the neutrons they diffract are captured on a two dimensional imaging detector. Their positions on the detector reveal their orientation whereas the projections themselves are used to reconstruct the shape of the grains. Indebted to established synchrotron diffraction contrast tomography, this 'cold neutron diffraction contrast tomography' is performed on recrystallized aluminium for experimental comparison between both. Differences between set-up and method are discussed, followed by the application range in terms of sample properties (crystallite size and number, mosaicity and typical materials). Neutron diffraction contrast tomography allows to study large grains in bulky metallic structures.

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Type
research article
DOI
10.1039/c4an01490a
Web of Science ID

WOS:000344310500019

Author(s)
Peetermans, S.
King, A.
Ludwig, W.
Reischig, P.
Lehmann, E. H.
Date Issued

2014

Publisher

Royal Society of Chemistry

Published in
Analyst
Volume

139

Issue

22

Start page

5765

End page

5771

Editorial or Peer reviewed

REVIEWED

Written at

EPFL

EPFL units
UPSWYG  
Available on Infoscience
December 30, 2014
Use this identifier to reference this record
https://infoscience.epfl.ch/handle/20.500.14299/109660
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