One-pot synthesis of functionalized bis(trifluoromethylated)benziodoxoles from iodine(i) precursors
Bis(trifluoromethylated)benziodoxoles (Bx) are broadly used cyclic hypervalent iodine reagents due to their stability and unique chemical properties. However, current methods to access them require several steps and long reaction times, making their synthesis tedious. Herein, a direct one-pot synthesis of bis(trifluoromethylated) Bx reagents from iodine(I) precursors is reported, enabling the synthesis of functionalized reagents.
CC2023_12637_GreenAccess1.pdf
preprint
openaccess
CC BY
11.91 MB
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f093c185cf8699cfde5e56a072bc046e
CC2023_12637_GreenAccess.pdf
postprint
embargo
2024-09-29
CC BY
11.93 MB
Adobe PDF
716a6f1392e61d17ab9e119c18754407